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[摘要]
用HPLC对桔红止咳冲剂中的柚皮甙作了定量分析、样品用甲醇提取,在VarianKYWGC187μm(220min×4.6mm)柱上,用甲醇-1%醋酸(33:67)作流动相,各成分能很好分离,以标准曲线法测定了不同批号的10批样品中柚皮甙的含量、结果表明本法简便、快速、重视性好,测定回收率达100.1%,RSD为1.18%。
[Key word]
[Abstract]
Quantitative analysis of naringin in Juhongzhike Chongji was carried out by HPLC. Samples were ex-traded with methanol. An ()DS column of Varian KYWG C18 7 μm(220×4.6 mm)and mobile phase methanol-1% acetic acid (33:67)were employed. Calibration curve method was used to determined the con-tents of naringin iu ten samples. Results showed that the method is simple,yuick and reproducible.The recov-ery was 100.1% and RSD 1.18%.
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