[关键词]
[摘要]
用高效液相色谱法测定清宫龙凤宝中淫羊藿甙的含量,采用 Spherisorb C18柱,4.6mm×150mm,流动相甲醇-水(50:50),流速1.0mL/min,检测波长270nm。测定结果平均回收率为101.38%,RSD=2.1%。
[Key word]
[Abstract]
A method for the determination of icarrin in Qinggonglongfenbao Oral Liquid by Rp-HPLC was described. A 150 mm ×4. 6 mm id. Spherisorb C18 column was used with.methanol-water(50: 50) as the mobile phase at a flowrate of 1. 0 mL/min and detected at 270 nm. The cefficient of icarrin was less than 2.2% and the recovery was more than 101. 0%. The method is simple, rapid, sensitive and of excellent precision.
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