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[摘要]
目的 培养布南色林的单晶,以验证所合成的化合物为布南色林。方法 通过温度、质量浓度、溶剂的考察,选择合适的条件,培养出大小适合X射线单晶衍射检测的布南色林单晶。结果 通过X射线单晶衍射测定,结果显示所得数据与文献报道一致,证明布南色林的化学结构正确。结论 采用本法可很好地获得大小适合X射线单晶衍射检测的布南色林单晶,并确证了其空间结构,提示合成的布南色林结构正确。
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[Abstract]
Objective To cultivate the single crystal of Blonanserin, and to establish the structure of Blonanserin. Method To selected the best condition by inspecting the different temperature, concentration, and solution. At this condition the single crystal size of Blonanserin fit for X-ray analysis. Results The structure of Blonanserin was accurate and the data was the same with the literature report. It proved that the structure of Blonanserin was right. Conclusion The single crystal size of Blonanserin obtained is fit for X-ray analysis and the space structure is proved right. And it suggests the structure that synthesized by our corporation be exact.
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