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[摘要]
赤芍以70%乙醇回流提取,减压浓缩,过大孔吸附树脂柱,先用水洗,再用20%乙醇洗脱,收集醇洗脱液,减压浓缩得赤芍总苷,收率为5.0%,其中芍药苷的含量占本品的75%以上。
[Key word]
[Abstract]
Technical conditions for the preparation of TPG were optimized. The root of Paeonia lacti flora Pall or P. vertchii Lynch were extracted with 70% ethanol under reflux. The concentrated extract was dissolved in water, passed through a macroporous resin column, and washed with water, and then eluated with 20% ethanol. Concentration of the eluate under reduced pressure gave the final TPG with a paeoniflorin content75%, and a recovery of 5. 0%.
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